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How to choose Viscometers


Concept of a Viscometer

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A viscometer is an instrument that quantifies the viscous resistance of a fluid by measuring the ratio of shear stress to shear rate under specified flow conditions.

Newtonian & Non-Newtonian Fluids

Newtonian fluids: Newtonian fluids are those whose viscosity, at any given temperature, does not change with shear rate (i.e., the rotational speed of the viscometer).

Non-Newtonian fluids: Their viscosity varies with shear rate (i.e., rotational speed) or shear time. They must be measured using a rotational viscometer or a rheometer, and multiple rotational speeds are required; otherwise, the data are incomplete.


Rotational Viscometers

A rotational viscometer is an instrument that measures the viscosity of a fluid by immersing a probe (called a rotor or spindle) into the sample and rotating it at a defined speed.
The fundamental principle is simple: the viscous drag of the fluid against the rotor produces a resistance (torque). The instrument measures this torque and converts it into a viscosity value using the known geometry of the rotor and the rotational speed.
It can measure both Newtonian and non-Newtonian fluids.


Special Types of Rotational Viscometers

Brookfield Viscometer (General-Purpose Type)

Offers a wide variety of spindles and accessories. It is suitable for measuring an extensive range of samples and for conducting in-depth rheological studies (such as generating rheological curves).

Krebs Stormer Viscometer (Industry-Specific Type)

Designed for the paint and coatings industry. Unlike other rotational viscometers that measure absolute viscosity in mPa·s (or cP), the Krebs Stormer viscometer measures the weight (grams) required to maintain a constant rotational speed of 200 RPM and then converts this value to Krebs Units (KU) using a specific logarithmic function.


Key Parameters of a Viscometer

Viscosity Measurement Range

Low Viscosity Range (1–1,000 mPa·s)

Characteristics: Flows very quickly, similar to water.

Typical materials: Water, milk, beverages, vegetable oil, low-viscosity engine oil, solvents.

Medium Viscosity Range (1,000–100,000 mPa·s)

Characteristics: Flows slowly.

Typical materials: Honey, syrup, paint, cream, lotion, shampoo, ketchup.

High Viscosity Range (above 100,000 mPa·s)

Characteristics: Hardly flows under its own weight.

Typical materials: Peanut butter, toothpaste, silicone, sealants, asphalt (in molten state), polymer melts.

Rotational Speed

Fixed speeds

(0.3, 0.6, 1.5, 3, 6, 12, 30, 60) r/min, or 6, 12, 30, 60, or 5, 10, 20, 50 RPM, or 200 RPM (Krebs Stormer).

Stepless speed control

0.1–200 RPM or 0.1–99.9 RPM or 1–60 RPM.


Viscometer Use

1. Selecting the Spindle

High-viscosity samples: Use a smaller spindle and a lower rotational speed. A small spindle has a smaller contact area and lower rotational resistance, preventing excessive torque and overrange errors.

Low-viscosity samples: Use a larger spindle and a higher rotational speed. A large spindle has a larger contact area, amplifying the torque signal and improving measurement accuracy.

2. Leveling the Instrument

Adjust the leveling feet on both sides of the instrument base so that the bubble in the spirit level is centered.

3. Instrument Settings

Select the spindle model and set the rotational speed (RPM).

Sample TypeRecommended Speed Selection
Low-viscosity samples (water, solvents, thin oils)High speed (60 rpm) + large spindle
Medium-viscosity samples (honey, cream)Medium speed (12–30 rpm) + medium spindle
High-viscosity samples (ointments, jam, toothpaste)Low speed (3–12 rpm) + small spindle

4. Temperature Control

Constant-temperature water bath (for viscometers without built-in temperature control):

Place the sample beaker in a water bath to heat or cool the sample until it reaches a stable temperature (e.g., 25°C, 40°C).

Heating chamber (for viscometers with built-in temperature control):

Heat the sample inside the instrument’s integrated heating chamber.

5. Validity of Measurement Values

The ideal torque range is 20%–80%.

Torque too low (<10%): Signal-to-noise ratio is poor, resulting in inaccurate data.

Torque too high (>80%): Approaches the instrument’s physical limit and may cause measurement errors.

Precautions

The sample must be free of air bubbles before measurement.

The liquid level must cover the spindle’s immersion line to ensure valid measurements.

The spindle must not touch the container walls during measurement.

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